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ACQUITY UPLC方法驗(yàn)證系統(tǒng)包

更新時(shí)間：2021-01-12

簡(jiǎn)要描述：

ACQUITY UPLC方法驗(yàn)證系統(tǒng)包
提供三批色譜填料（來(lái)自不同批次的顆粒基體）以判斷一個(gè)分析方法的耐受性，可靠性和一致性。

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ACQUITY UPLC方法驗(yàn)證系統(tǒng)包

UPLC方法驗(yàn)證包— 確保方法耐用性

 

 

為了確保分析方法持續(xù)可靠且具有重現(xiàn)性，采用多批色譜填料進(jìn)行檢測(cè)和驗(yàn)證變得尤為重要。作為硅膠雜化顆粒的主要生產(chǎn)商，沃特世公司為不同批次之間的重現(xiàn)性設(shè)立了行業(yè)的基準(zhǔn)?；谛抛u(yù)*的顆粒和色譜柱生產(chǎn)的過(guò)程控制，使批與批和柱與柱之間的變異性小化，從而為分析方法長(zhǎng)期的可靠性提供信心。

 

ACQUITY UPLC方法驗(yàn)證包提供三批色譜填料(來(lái)自不同批次的顆?；w)以判斷一個(gè)分析方法的耐受性，可靠性和一致性。

來(lái)自三個(gè)不同批次的填料基體的三個(gè)不同批次的鍵合處理的ACQUITY UPLC柱對(duì)氯氨平有關(guān)物質(zhì)的分析表現(xiàn)出zhuo越的重現(xiàn)性，保證了分析方法的長(zhǎng)期重現(xiàn)性。

選擇性(a)
批號(hào)雜質(zhì)C雜質(zhì)A氯氨平雜質(zhì)B
1191.031.071.071.59
1201.031.071.071.58
1241.021.071.071.58

 

 

ACQUITY UPLC方法驗(yàn)證系統(tǒng)包

訂貨信息：

ACQUITY UPLC方法開(kāi)發(fā)套裝[MDK: Method Development Kit]

套裝名稱數(shù)量固定相顆粒大小配置部件編號(hào)
選擇性*大化大化UPLC方法開(kāi)發(fā)套裝：寬泛的選擇性用于方法開(kāi)發(fā)，包括在低pH和高pH下。是低離子強(qiáng)度添加劑條件時(shí)(例如甲酸)的*佳佳選擇
選擇性*大化UPLC方法開(kāi)發(fā)套裝4件/包CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SBCSH 1.7 μm; HSS 1.8 μm2.1 x 50 mm176002123
選擇性*大化UPLC方法開(kāi)發(fā)套裝4件/包CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SBCSH 1.7 μm; HSS 1.8 μm2.1 x 100 mm176002124
選擇性*大化UPLC方法開(kāi)發(fā)套裝4件/包CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SBCSH 1.7 μm; HSS 1.8 μm3.0 x 50 mm176002125
選擇性*大化UPLC方法開(kāi)發(fā)套裝4件/包CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SBCSH 1.7 μm; HSS 1.8 μm3.0 x 100 mm176002126
高&低pH，寬選擇性的UPLC色譜柱套裝：通過(guò)開(kāi)拓低和高流動(dòng)相pH使分離選擇性寬
高&低pH，寬選擇性的UPLC色譜柱套裝4件/包BEH C18, BEH C8, BEH Shield RP18,   BEH苯基BEH 1.7 μm2.1 x 50 mm176001042
高&低pH，寬選擇性的UPLC色譜柱套裝4件/包BEH C18, BEH C8, BEH Shield RP18,   BEH苯基BEH 1.7 μm2.1 x 100 mm176001043
高&低pH，寬選擇性的UPLC色譜柱套裝4件/包BEH C18, BEH C8, BEH Shield RP18,   BEH苯基BEH 1.7 μm3.0 x 50 mm176001881
高&低pH，寬選擇性的UPLC色譜柱套裝4件/包BEH C18, BEH C8, BEH Shield RP18,   BEH苯基BEH 1.7 μm3.0 x 100 mm176001882
UPLC方法開(kāi)發(fā)套裝：通過(guò)開(kāi)拓低和高流動(dòng)相pH(BEH色譜柱)將分離選擇性*大化大化和適用于極性化合物保留性(HSS   T3)
UPLC方法開(kāi)發(fā)套裝4件/包BEH C18, BEH Shield RP18, BEH 苯基, HSS   T3BEH 1.7 μm; HSS 1.8 μm2.1 x 50 mm176001603
UPLC方法開(kāi)發(fā)套裝4件/包BEH C18, BEH Shield RP18, BEH 苯基, HSS   T3BEH 1.7 μm; HSS 1.8 μm2.1 x 100 mm176001604
UPLC方法開(kāi)發(fā)套裝4件/包BEH C18, BEH Shield RP18, BEH 苯基, HSS   T3BEH 1.7 μm; HSS 1.8 μm3.0 x 50 mm176001883
UPLC方法開(kāi)發(fā)套裝4件/包BEH C18, BEH Shield RP18, BEH 苯基, HSS   T3BEH 1.7 μm; HSS 1.8 μm3.0 x 100 mm176001884
L1   UPLC色譜柱套裝：依從USP藥典中L1類別，但提供不同硅醇基活性和疏水性的C18色譜柱
L1 UPLC色譜柱套裝4件/包BEH C18, BEH Shield RP18, HSS C18, HSS   T3BEH 1.7 μm; HSS 1.8 μm2.1 x 50 mm176001605
L1 UPLC色譜柱套裝4件/包BEH C18, BEH Shield RP18, HSS C18, HSS   T3BEH 1.7 μm; HSS 1.8 μm2.1 x 100 mm176001606
L1 UPLC色譜柱套裝4件/包BEH C18, BEH Shield RP18, HSS C18, HSS   T3BEH 1.7 μm; HSS 1.8 μm3.0 x 50 mm176001885
L1 UPLC色譜柱套裝4件/包BEH C18, BEH Shield RP18, HSS C18, HSS   T3BEH 1.7 μm; HSS 1.8 μm3.0 x 100 mm176001886
質(zhì)譜UPLC色譜柱套裝：直鏈烷烴C18柱，具有不同的硅醇活性、峰形、選擇性和疏水性，且無(wú)MS流失問(wèn)題
質(zhì)譜UPLC色譜柱套裝4件/包BEH C18, HSS C18, HSS T3, HSS C18 SBBEH 1.7 μm; HSS 1.8 μm2.1 x 50 mm176001607
質(zhì)譜UPLC色譜柱套裝4件/包BEH C18, HSS C18, HSS T3, HSS C18 SBBEH 1.7 μm; HSS 1.8 μm2.1 x 100 mm176001608
質(zhì)譜UPLC色譜柱套裝4件/包BEH C18, HSS C18, HSS T3, HSS C18 SBBEH 1.7 μm; HSS 1.8 μm3.0 x 50 mm176001887
質(zhì)譜UPLC色譜柱套裝4件/包BEH C18, HSS C18, HSS T3, HSS C18 SBBEH 1.7 μm; HSS 1.8 μm3.0 x 100 mm176001888
低pH，寬選擇性UPLC色譜柱套裝：有各種不同的鍵合相和選擇性，用于開(kāi)發(fā)低pH流動(dòng)相條件下的反相方法
低pH，寬選擇性UPLC色譜柱套裝4件/包BEH Shield RP18, BEH 苯基, HSS C18, HSS   C18 SBBEH 1.7 μm; HSS 1.8 μm2.1 x 50 mm176001609
低pH，寬選擇性UPLC色譜柱套裝4件/包BEH Shield RP18, BEH 苯基, HSS C18, HSS   C18 SBBEH 1.7 μm; HSS 1.8 μm2.1 x 100 mm176001610
低pH，寬選擇性UPLC色譜柱套裝4件/包BEH Shield RP18, BEH 苯基, HSS C18, HSS   C18 SBBEH 1.7 μm; HSS 1.8 μm3.0 x 50 mm176001889
低pH，寬選擇性UPLC色譜柱套裝4件/包BEH Shield RP18, BEH 苯基, HSS C18, HSS   C18 SBBEH 1.7 μm; HSS 1.8 μm3.0 x 100 mm176001890
選擇性*大化大化的RP 和 HILIC   UPLC方法開(kāi)發(fā)套裝：通過(guò)綜合HILIC和RP固定相以提供寬分離選擇性，用以保留分離跨越寬泛極性范圍的分析物
選擇性*大化的RP 和   HILIC UPLC方法開(kāi)發(fā)套裝4件/包CSH C18, CSH苯己基, CSH氟苯基, BEH AmideCSH 1.7 μm; BEH 1.7 μm2.1 x 50 mm176002127
選擇性*大化的RP 和   HILIC UPLC方法開(kāi)發(fā)套裝4件/包CSH C18, CSH苯己基, CSH氟苯基, BEH AmideCSH 1.7 μm; BEH 1.7 μm2.1 x 100 mm176002128
選擇性*大化的RP 和   HILIC UPLC方法開(kāi)發(fā)套裝4件/包CSH C18, CSH苯己基, CSH氟苯基, BEH AmideCSH 1.7 μm; BEH 1.7 μm3.0 x 50 mm176002129
選擇性*大化的RP 和   HILIC UPLC方法開(kāi)發(fā)套裝4件/包CSH C18, CSH苯己基, CSH氟苯基, BEH AmideCSH 1.7 μm; BEH 1.7 μm3.0 x 100 mm176002130
UPLC   RP和HILIC方法開(kāi)發(fā)套裝：通過(guò)綜合RP和HILIC固定相以提供寬分離選擇性，用以保留分離跨越寬泛極性范圍的分析物
UPLC RP和HILIC   方法開(kāi)發(fā)套裝4件/包BEH C18, BEH Shield RP18, BEH Amide,   HSS C18 SBBEH 1.7 μm; HSS 1.8 μm2.1 x 50 mm176001959
UPLC RP和HILIC   方法開(kāi)發(fā)套裝4件/包BEH C18, BEH Shield RP18, BEH Amide,   HSS C18 SBBEH 1.7 μm; HSS 1.8 μm2.1 x 100 mm176001960
UPLC RP和HILIC   方法開(kāi)發(fā)套裝4件/包BEH C18, BEH Shield RP18, BEH Amide,   HSS C18 SBBEH 1.7 μm; HSS 1.8 μm3.0 x 50 mm176001961
UPLC RP和HILIC   方法開(kāi)發(fā)套裝4件/包BEH C18, BEH Shield RP18, BEH Amide,   HSS C18 SBBEH 1.7 μm; HSS 1.8 μm3.0 x 100 mm176001962
UPLCHILIC方法開(kāi)發(fā)套裝：在低pH(對(duì)堿性分析物)和高pH(對(duì)酸性分析物)下為極性和/或可離子化化合物輕松開(kāi)發(fā)HILIC方法
UPLCHILIC方法開(kāi)發(fā)套裝4件/包BEH Amide, BEH HILICBEH 1.7 μm2.1 x 50 mm176001963
UPLCHILIC方法開(kāi)發(fā)套裝4件/包BEH Amide, BEH HILICBEH 1.7 μm2.1 x 100 mm176001964
UPLCHILIC方法開(kāi)發(fā)套裝4件/包BEH Amide, BEH HILICBEH 1.7 μm3.0 x 50 mm176001965
UPLCHILIC方法開(kāi)發(fā)套裝4件/包BEH Amide, BEH HILICBEH 1.7 μm3.0 x 100 mm176001966

 

 

ACQUITY UPLC方法轉(zhuǎn)換套裝[MTK: Method Transfer Kit]*

套裝名稱UPLC Column 2.1 mm IDHPLC Column 4.6 mm ID部件編號(hào)
CSH C18 1.7 to   5 μm MTK50 mm, 1.7 μm150 mm, 5 μm186005529
CSH   Phenyl-Hexyl 1.7 to 5 μm MTK50 mm, 1.7 μm150 mm, 5 μm186005530
CSH   Fluoro-Phenyl 1.7 to 5 μm MTK50 mm, 1.7 μm150 mm, 5 μm186005531
BEH C18 1.7 to   5 μm MTK50 mm, 1.7 μm150 mm, 5 μm186004958
BEH Shield   RP18 1.7 to 5 μm MTK50 mm, 1.7 μm150 mm, 5 μm186004959
BEH HILIC 1.7   to 5 μm MTK50 mm, 1.7 μm150 mm, 5 μm186004960
HSS C18 1.8 to   5 μm MTK50 mm, 1.8 μm150 mm, 5 μm186004961
HSS T3 1.8 to   5 μm MTK50 mm, 1.8 μm150 mm, 5 μm186004962
HSS C18 SB 1.8   to 5 μm MTK50 mm, 1.8 μm150 mm, 5 μm186004963
HSS Cya.8   to 5 μm MTK50 mm, 1.8 μm150 mm, 5 μm186005979
HSS PFP 1.8 to   5 μm MTK50 mm, 1.8 μm150 mm, 5 μm186006000
CSH C18 1.7 to   3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186005532
CSH   Phenyl-Hexyl 1.7 to 3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186005533
CSH   Fluoro-Phenyl 1.7 to 3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186005534
BEH C18 1.7 to   3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186004964
BEH Shield   RP18 1.7 to 3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186004965
BEH HILIC 1.7   to 3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186004966
BEH Amide 1.7   to 3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186004967
HSS C18 1.8 to   3.5 μm MTK50 mm, 1.8 μm100 mm, 3.5 μm186004968
HSS T3 1.8 to   3.5 μm MTK50 mm, 1.8 μm100 mm, 3.5 μm186004969
HSS C18 SB 1.8   to 3.5 μm MTK50 mm, 1.8 μm100 mm, 3.5 μm186004970
HSS Cya.8   to 3.5 μm MTK50 mm, 1.8 μm100 mm, 3.5 μm186005980
HSS PFP 1.8 to   3.5 μm MTK50 mm, 1.8 μm100 mm, 3.5 μm186006001
CSH C18 1.7 to   3.5 μm High Rs MTK100 mm, 1.7 μm150 mm, 3.5 μm186005535
CSH   Phenyl-Hexyl 1.7 to 3.5 μm高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186005536
CSH   Fluoro-Phenyl 1.7 to 3.5 μm高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186005537
BEH C18 1.7 to   3.5 μm 高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004971
BEH Shield   RP18 1.7 to 3.5 μm高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004972
BEH HILIC 1.7   to 3.5 μm 高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004973
BEH Amide 1.7   to 3.5 μm 高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004974
HSS C18 1.8 to   3.5 μm 高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004975
HSS T3 1.8 to   3.5 μm 高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004976
HSS C18 SB 1.8   to 3.5 μm 高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004977
HSS Cya.8   to 3.5 μm 高分辨 MTK100 mm, 1.8 μm150 mm, 3.5 μm186005981
HSS PFP 1.8 to   3.5 μm 高分辨 MTK100 mm, 1.8 μm150 mm, 3.5 μm186006002

*每個(gè)套裝都含有一根UPLC色譜柱和一根HPLC色譜柱，可從ACQUITY UPLC在線社區(qū)
www.waters。。ｃｏｍ/myuplc下載ACQUITY UPLC Columns Calculator用于計(jì)算方法轉(zhuǎn)移。

 

 

ACQUITY UPLC方法驗(yàn)證套裝[MVK:Method Validation Kit]**

固定相粒徑色譜柱長(zhǎng)度部件編號(hào) 2.1 mm ID部件編號(hào) 3.0 mm ID
CSH C181.7 μm50 mm186005571186005573
CSH C181.7 μm100 mm186005572186005574
CSH 苯己基1.7 μm50 mm186005579186005581
CSH 苯己基1.7 μm100 mm186005580186005582
CSH 氟苯基1.7 μm50 mm186005575186005577
CSH 氟苯基1.7 μm100 mm186005576186005578
BEH C181.7 μm50 mm186004044186004691
BEH C181.7 μm100 mm186004045186004692
BEH C81.7 μm50 mm186004046186004693
BEH C81.7 μm100 mm186004047186004694
BEH Shield   RP181.7 μm50 mm186004048186004695
BEH Shield   RP181.7 μm100 mm186004049186004696
BEH Phenyl1.7 μm50 mm186004050186004697
BEH Phenyl1.7 μm100 mm186004052186004698
BEH HILIC1.7 μm50 mm186004053186004699
BEH HILIC1.7 μm100 mm186004054186004700
BEH Amide1.7 μm50 mm186004807186004809
BEH Amide1.7 μm100 mm186004808186004810
BEH130 C181.7 μm100 mm186004896-
BEH300 C181.7 μm100 mm186004897-
BEH300 C41.7 μm100 mm186004899-
寡核苷酸 C181.7 μm100 mm186004898-
Glycan BEH   Amide1.7 μm100 mm186004907-
HSS T31.8 μm50 mm186004055186004701
HSS T31.8 μm100 mm186004056186004702
HSS C181.8 μm50 mm186004057186004703
HSS C181.8 μm100 mm186004058186004704
HSS C 18 SB1.8 μm50 mm186004137186004705
HSS C 18 SB1.8 μm100 mm186004138186004709
HSS PFP1.8 μm50 mm186005975-
HSS PFP1.8 μm100 mm186005976-
HSS PFP1.8 μm50 mm186005977-
HSS PFP1.8 μm100 mm186005978-
HSS 氰基1.8 μm50 mm186005996186005998
HSS 氰基1.8 μm100 mm186005997186005999

**每個(gè)套裝包括來(lái)自3個(gè)不同批次填料的3根色譜柱。

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